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Beilstein J. Org. Chem. 2016, 12, 192–197, doi:10.3762/bjoc.12.21
Graphical Abstract
Scheme 1: Direct fluorination of 1,2-bis(3-nitrophenyl)disulfane.
Scheme 2: Direct fluorination of 3-nitro-1-(pentafluorosulfanyl)benzene (1).
Figure 1: Conversion vs added fluorine equivalents for the fluorination of 1 in MeCN (left) and anhydrous HF ...
Scheme 3: Preparative fluorination of 3-nitro-1-(pentafluorosulfanyl)benzene (1).
Scheme 4: Synthesis of 2 by fluorodenitration of 5.